Brauer Handbuch Der Prparativen Anorganischen Chemietek
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(C 5H 4CH 2CH 2CH 2C 5H 4)Sm(THF) 2 ( 1) has been obtained as purple crystals by treatment of SmCl 2 with Na 2(C 5H 4CH 2CH 2CH 2C 5H 4) in tetrahydrofuran (THF). The corresponding ytterbium compound 2 results from the analogous reaction using YbCl 2 or from the reduction of (C 5H 4CH 2CH 2CH 2C 5H 4)YbCl(THF) ( 3) with Na/Hg in THF. The structure of 2 has been determined by an X-ray diffraction study. The crystals are orthorhombic, space group Fdd2, with a 2938(3), b 3190(7), c 817.8(8) pm, Z = 16, ρ calc.
1.69 g/cm 3, R = 0.0454 for 1727 observed data ( F o ⩾ 4σ( F o)). • Previous article in issue • Next article in issue.
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VC~: Brauer G. ~andbuch der Pra. 2002(4) 3.Arehart S V;Matyjaszewski K 查看详情[外文期刊] 1999(07) 4.Brauer G Handbuch der Prparativen Chemie.Ⅱ Band. Theories of gravitation.
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